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Topics in Chemical Engineering
A series edited by R. Hughes, University of Salford, U.K.

Volume 1

HEAT AND MASS TRANSFER IN PACKED BEDS by N. Wakao and S. Kaguei THREE-PHASE CATALYTIC REACTORS by P.A. Ramachandran and R.V. Chaudhari DRYING: PRINCIPLES, APPLICATIONS AND DESIGN . by Cz. Strumillo and T. Kudra T H E ANALYSIS OF CHEMICALLY REACTING SYSTEMS: A Stochastic Approach by L.K.Doraiswamy and B.D. Kulkarni CONTROL OF LIQUID-LIQUID EXTRACTION COLUMNS by K. Najim . CHEMICAL ENGINEERING DESIGN PROJECT . A Case Study Appidach by M.S. Rayn and D.W. Johnston ,

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CHEMICAL ENGINEERING DESIGN PROJECT
A Case Study Approach

By Martyn S. Ray
Curtin University of Technology, Western Australia
and

David W. Johnston
Shell Refining (Australia) Pty. Ltd., A

BIBLIOTECA

CUCEI

CENTRAL

No. DE ADQUISICION

016722

FECHA ENTREGA CLASIFIACION
0.GORDON AND BREACH SCIENCE PUBLISHERS New York London Paris Montreux Tokyo Melbourne

01989 by OPA (Amsterdam) B.V. All rights reserved. Published under license by Gordon and Breach Science Publishers S.A. Gordon and Breach Science Publishers Post Office Box 786 Cooper Station New York, New York 10276 United States of America Post Office Box 197 London WC2E 9PX England

58, rue Lhomond 75005Paris France

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Private Bag 8 Camberwell, Victoria 3 124 Australia

Library of Congress Cataloging-in-Publication Data Ray, Martyn S., 1949Chemical engineering design project : a case study approach / by Martin S. Ray and David W. Johnston. P. cm. - (Topics in chemical engineering, ISSN 0277-5883 ; v. 5)Bibliography: p. Includes index. ISBN 2-88124713-X. -1SBN 2-88124-712-l (pbk.) 1. Chemical engineering-Case studies. 2. Nitric acid. I. Johnston, David W., 1964 . II. Title. III. Series. TP149.R35 1989 89-2171 6606~20 CIP No part of this book may be reproduced or utilized in any form or by any means, electronic or mechanical, including photocoping and recording, or by any information storage orretrieval system, without permission in writing from the publishers. Printed in Great Britain by Bell and Bain Ltd., Glasgow

Contents
Introduction to the Series Acknowledgements I About this Book - The Case Study Approach II Advice to the Student III To the Lecturer IV The Scope of Design Projects V Effective Communications VI Comments on the Case Study Approach
The Case Study - Summary for theCompleted Project PART I PRELIMINARY DESIGN - TECHNICAL AND ECONOMIC FEASIBILITY CHAPTER 1 THE DESIGN PROBLEM
x111

xiv xv xvii xix xxi xxii xxiv xxv 1 3 3 4

1.1

Initial Considerations and Specification

The Case Study - Summary for Part I Feasibility Study and Initial Design Considerations 1.2 Case Study- Defining the Problem and Background Information Summary 1.2.1 Introduction 1.2.2Properties and Uses 1.2.3 The Evolution of Nitric Acid Production Processes 1.2.4 Ammonia Oxidation Chemistry
V

7 9

vi

CONTENTS
12 12

CHAPTER 2 FEASIBILITY STUDY AND LITERATURE SURVEY 2.1 Initial Feasibility Study Presentation of Literature Surveys for Projects 2.2
2.3 Case Study- Feasibility Study (Market Assessment) Summary 2.3.1 Introduction 2.3.2 The Domestic Scene 2.3.3 TheGlobal Market 2.3.4 Market Analysis Discussion 2.3.5 Market Assessment Conclusions Case Study - Literature Survey Summary 2.4.1 Introduction 2.4.2 General Information 2.4.3 Process Technology 2.4.4 Cost Estimation 2.4.5 Market Data 2.4.6 Thermodynamic Data Case Study - Bibliography

15
21 21 22 22 24 24 27 28 28 29 29 30 31 32 33 33 37 37 40 40 41 42 45 46 46 47

2.4

2.5

CHAPTER 3 PROCESS...
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