Destilaciobach

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  • Publicado : 8 de enero de 2012
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Anexo 1: Datos tomados en el laboratorio

Tabla 1.1. Condiciones de la alimentación.
Alimentación (mL) | 5000 |
ρa (g/mL) | 0,9798 |
Za | 0,0509 |

Tabla 1.2. Datos de las muestras tomadas experimentalmente.
N° | V (mL) | Tiempo (s) | ρ fondo (g/mL) | ρ tope (g/mL) | L/D | T Fondo (°C) | T tope (°C) |
1 | 50 | 464 | 0,9841 | 0,8335 | 0,3 | 86,0 | 73 |
2 | 50 | 476 | 0,9874 |0,8275 | 0,3 | 87,0 | 73 |
3 | 50 | 444 | 0,9887 | 0,833 | 0,3 | 87,0 | 73 |
4 | 50 | 420 | 0,9891 | 0,8283 | 0,3 | 88,0 | 73 |
5 | 50 | 458 | 0,989 | 0,8321 | 0,4 | 89,0 | 73 |
6 | 50 | 300 | 0,9912 | 0,8299 | 0,67 | 90,0 | 73 |
7 | 50 | 313 | 0,992 | 0,8294 | 0,67 | 91,0 | 73 |
8 | 50 | 300 | 0,9941 | 0,83 | 1,00 | 91,0 | 73 |
9 | 50 | 287 | 0,9913 | 0,8305 | 1,00 | 92,0 | 75 |
10 |50 | 354 | 0,9904 | 0,8634 | 1,00 | 92,0 | 83 |
11 | 50 | 555 | 0,9923 | 0,8927 | 0,50 | 93,0 | 86 |
12 | 50 | 808 | 0,9924 | 0,9148 | 0,2 | 93,0 | 87 |

Tabla 1.3. Datos del producto de tope obtenido.
Destilado (mL) | 550 |
ρ destilado | 0,8649 |

Tabla 1.4. Datos del producto de fondo obtenido.
Fondo (mL) | 4405 |
ρb | 0,9924 |

Anexo 2: Resultados obtenidos:

Tabla 2.1.Condiciones de equilibrio líquido-vapor.
X1 | X2 | γ1 | γ2 | Y1 | Y2 | Pv(1) | Pv(2) | T |
0,0000 | 1,0000 | 5,3645 | 1,0000 | 0,0000 | 1,0000 | 0,0000 | 667,0000 | 95,2000 |
0,0200 | 0,9800 | 4,7665 | 1,0012 | 0,1797 | 0,8203 | 1257,3072 | 557,6472 | 91,5780 |
0,0400 | 0,9600 | 4,2686 | 1,0046 | 0,2862 | 0,7138 | 1118,0739 | 493,6654 | 88,3794 |
0,0600 | 0,9400 | 3,8507 | 1,0101 | 0,3560 |0,6440 | 1027,8688 | 452,3897 | 86,1262 |
0,0800 | 0,9200 | 3,4974 | 1,0174 | 0,4050 | 0,5950 | 965,5814 | 423,9758 | 84,4726 |
0,1000 | 0,9000 | 3,1967 | 1,0265 | 0,4412 | 0,5588 | 920,5357 | 403,4741 | 83,2206 |
0,1200 | 0,8800 | 2,9390 | 1,0372 | 0,4689 | 0,5311 | 886,7659 | 388,1314 | 82,2481 |
0,1400 | 0,8600 | 2,7171 | 1,0494 | 0,4908 | 0,5092 | 860,6870 | 376,2994 | 81,4758 |0,1600 | 0,8400 | 2,5247 | 1,0631 | 0,5087 | 0,4913 | 840,0226 | 366,9342 | 80,8499 |
0,1800 | 0,8200 | 2,3573 | 1,0781 | 0,5237 | 0,4763 | 823,2646 | 359,3464 | 80,3328 |
0,2000 | 0,8000 | 2,2107 | 1,0945 | 0,5365 | 0,4635 | 809,3801 | 353,0644 | 79,8978 |
0,2200 | 0,7800 | 2,0820 | 1,1121 | 0,5478 | 0,4522 | 797,6427 | 347,7573 | 79,5251 |
0,2400 | 0,7600 | 1,9685 | 1,1308 | 0,5578 | 0,4422 |787,5307 | 343,1877 | 79,2003 |
0,2600 | 0,7400 | 1,8679 | 1,1508 | 0,5670 | 0,4330 | 778,6635 | 339,1825 | 78,9127 |
0,2800 | 0,7200 | 1,7786 | 1,1718 | 0,5755 | 0,4245 | 770,7598 | 335,6141 | 78,6540 |
0,3000 | 0,7000 | 1,6990 | 1,1939 | 0,5835 | 0,4165 | 763,6095 | 332,3871 | 78,4180 |
0,3200 | 0,6800 | 1,6279 | 1,2171 | 0,5912 | 0,4088 | 757,0550 | 329,4301 | 78,2001 |
0,3400 |0,6600 | 1,5641 | 1,2412 | 0,5988 | 0,4012 | 750,9773 | 326,6891 | 77,9966 |
0,3600 | 0,6400 | 1,5069 | 1,2664 | 0,6061 | 0,3939 | 745,2865 | 324,1235 | 77,8048 |
0,3800 | 0,6200 | 1,4553 | 1,2926 | 0,6135 | 0,3865 | 739,9151 | 321,7025 | 77,6227 |
0,4000 | 0,6000 | 1,4089 | 1,3196 | 0,6208 | 0,3792 | 734,8119 | 319,4031 | 77,4486 |
0,4200 | 0,5800 | 1,3669 | 1,3477 | 0,6283 | 0,3717 |729,9392 | 317,2081 | 77,2815 |
0,4400 | 0,5600 | 1,3289 | 1,3766 | 0,6358 | 0,3642 | 725,2690 | 315,1050 | 77,1204 |
0,4600 | 0,5400 | 1,2946 | 1,4064 | 0,6435 | 0,3565 | 720,7812 | 313,0844 | 76,9648 |
0,4800 | 0,5200 | 1,2634 | 1,4372 | 0,6514 | 0,3486 | 716,4616 | 311,1401 | 76,8143 |
0,5000 | 0,5000 | 1,2351 | 1,4687 | 0,6595 | 0,3405 | 712,3010 | 309,2678 | 76,6685 |
0,5200 | 0,4800 |1,2094 | 1,5012 | 0,6678 | 0,3322 | 708,2936 | 307,4648 | 76,5275 |
0,5400 | 0,4600 | 1,1861 | 1,5345 | 0,6765 | 0,3235 | 704,4365 | 305,7299 | 76,3912 |
0,5600 | 0,4400 | 1,1649 | 1,5687 | 0,6854 | 0,3146 | 700,7292 | 304,0627 | 76,2595 |
0,5800 | 0,4200 | 1,1457 | 1,6036 | 0,6946 | 0,3054 | 697,1726 | 302,4636 | 76,1326 |
0,6000 | 0,4000 | 1,1283 | 1,6394 | 0,7041 | 0,2959 | 693,7693 |...
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